By John Comyn
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2 Force needed to remove steel cylinder from adhesives used with paper. Force (N) Adhesive Untreated Water 20 PPm Zirconium acetate Pressure-sensitive acrylic E t h ylene-vin yl-ace ta te hot me1t 264 2 36 73 220 23 -~ -- ~ ~ _ _ _ _ _ _ _ ~~ ~~~ 7 - ~~ ~~~ Zirconium compounds can also reduce adhesion, and this is exploited during the reclamation of waste paper, where adhesives of the many kinds can be present, causing problems by adhering to the processing machinery and producing unsightly spots on the final product.
Component Parts by weight Methyl methacrylate Methacrylic acid Ethylene glycol dimethacry late Chlorosulfonated polyethylene Cumene hydroperoxide N,N-dimethylaniline 85 15 2 100 6 2 ANAEROBIC ADHESIVES Anaerobic adhesives cure in the absence of oxygen, which inhibits polymerization. They are usually based on dimethacrylates of polyethylene glycol, but end-capped polyurethanes are also used. They contain a redox free-radical initiator, and are usually supplied in air permeable polyethylene containers only partially filled, to maintain an adequate supply of oxygen.
Hysol EA 2989. This has the advantages of being water-based and not containing chromium, even though it is corrosion inhibiting. It is formulated for use with Hysol EA 9689 epoxide film adhesive. The recommended coating thickness is 5-10 pm and the primer is dried in air for at least 1 h, and then cured for 1 h at 175°C. 3M EC-2320. This is particularly recommended for AF-111, AF-126 and AF-126-2 film adhesives; it improves shear and peel strengths and environmental resistance. 1 pm. It can be dried at temperatures up to 120°C and primed surfaces have a 90 day shelf-life.